发明名称 PREPARATION OF 4-HYDROXYTHIOPHENOL
摘要 PURPOSE:To obtain the titled compound by a simple operation in high yield industrially advantageously, by reducing 4-hydroxybenzenesulfonyl chloride. CONSTITUTION:4-Hydroxybenzenesulfonyl chloride is reduced using a reducing agent of zinc/hydrochloric acid or zinc/sulfuric acid, the desired substance is extracted from the prepared reaction product by the use of an organic acid, etc., and it is purified by a conventional procedure, to give the desired substance. EFFECT:Multi-stage batch-wise reduction can be carried out by adding further a reducing agent to an extract of a reduction product with a solvent, consequently, yield is further improved.
申请公布号 JPS59193868(A) 申请公布日期 1984.11.02
申请号 JP19830068057 申请日期 1983.04.18
申请人 RICOH KK 发明人 MARUYAMA KATSUJI;HIGETA SHIGERU
分类号 C07C319/14;C07C67/00;C07C313/00;C07C323/20 主分类号 C07C319/14
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