发明名称 PROCESS FOR PRODUCING 5-BROMO-5-NITRO-2-ALKYL SUBSTITUTED-1,3-DIOXANE
摘要 Title compound (I ; R = Me, Et. Pr. Me2CH), useful as fungicide in lower concn., which has stable solubility in mineral oil and water and under alkali concns. were prepd. by reacting 2-bromo-2-nitropropane-1,3-diol with aldehyde in benzen contg P-toluene sulphonic acid, stirring acid, stirring the mixt. for 30 min., filtrating the soln., evaporating the filtrate on a rotary evaporator at 45≦̸C, and distg. the oily residue under vacuum. The yield was 85%.
申请公布号 KR790000164(B1) 申请公布日期 1979.03.24
申请号 KR19740001506 申请日期 1974.02.15
申请人 ELI LILLY AND CO 发明人 LEWIS CHRISTOPHER LAPPAS;CLARENCE AUGUST HIRSCH
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