发明名称 METHOD FOR PRODUCING EMISSIVE MATERIAL FOR OXIDE CATHODES
摘要 FIELD: electronic engineering. SUBSTANCE: emissive material for oxide cathodes of vacuum tubes and gas-discharge devices based on composite compounds of alkali-earth metals (Ba, Sr, and Ca) is produced by using method that involves deposition of difficult-to-dissolve compounds of alkali-earth metals out of aqueous solutions of their nitrates with solution of ammonium oxalate and ammonium carbonate mixture having mole proportion (NH4)2C2O4:(NH4)2CO3 = 0,3÷0,7:0,7÷0,3. Deposits obtained are separated from mother liquor by means of Buchner funnel, rinsed with distilled water, and dried out at 100-150 C for 10 h. As an alternative, they may be vacuum dried at temperature of 240-250 C and residual pressure of 5.10-2 - 1.10-2 tors. Material is designed to improve operating and other characteristics of vacuum tubes and gas-discharge devices using them. EFFECT: improved emissive capability and emissive uniformity of material. 1 tbl, 6 ex
申请公布号 RU2149480(C1) 申请公布日期 2000.05.20
申请号 RU19990100194 申请日期 1999.01.05
申请人 IVANOVSKIJ GOSUDARSTVENNYJ KHIMIKO-TEKHNOLOGICHESK;IJ UNI 发明人 ALEKSANDROV E.M.;GORFINKEL' B.I.;NOGTEV G.A.;OVCHINNIKOV N.L.;SHOFMAN G.S.
分类号 H01J9/04;H01J19/06;(IPC1-7):H01J9/04 主分类号 H01J9/04
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