发明名称 METHOD FOR PRODUCING 1,1,1,3,3,3-HEXAFLUORO-tert-BUTANOL
摘要 PROBLEM TO BE SOLVED: To provide an efficient method for producing 1,1,1,3,3,3-hexafluoro-tert-butanol (abbreviation: HFTB).SOLUTION: The method for producing HFTB at least comprises a first step to a third step. The first step: a step of contacting a first mixture at least containing HFTB and one or more ether type solvent selected from the group consisting of diethyl ether, tetrahydrofuran, 2-methyltetrahydrofuran, diethoxymethane, and dimethoxymethane with an alkali metal base to obtain a second mixture at least containing an alkali metal 1,1,1,3,3,3-hexafluoro-tert-butoxide and the ether solvent. The second step: a step of separating the ether type solvent from the second mixture obtained in the first step. The third step: a step of obtaining HFTB by contacting the second mixture after the second step with an acid.
申请公布号 JP2015193589(A) 申请公布日期 2015.11.05
申请号 JP20150034717 申请日期 2015.02.25
申请人 CENTRAL GLASS CO LTD 发明人 MURAKAWA JUNJI;AKIBA SHINYA;NADANO RYO
分类号 C07C29/92;C07C29/40;C07C31/38 主分类号 C07C29/92
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