发明名称 α−アミノ−ε−カプロラクタムの製造方法
摘要 <p><P>PROBLEM TO BE SOLVED: To provide a method for producingα-amino-ε-caprolactam from lysine or a salt thereof by using a nonpolar solvent which is easily recovered and recycled in place of a polar solvent such as an alcohol. <P>SOLUTION: The problem is solved by the method for producingα-amino-ε-caprolactam, in which lysine or a salt thereof is dehydrated and cyclized in the presence of the mixed solvent of the nonpolar solvent and water kept at a temperature of 200-400°C and a pressure of 5-40 MPa. An amount of water to be used is reduced, and corrosion of a reactor is alleviated, and the nonpolar solvent is easily recovered and recycled. <P>COPYRIGHT: (C)2012,JPO&INPIT</p>
申请公布号 JP5776194(B2) 申请公布日期 2015.09.09
申请号 JP20110021744 申请日期 2011.02.03
申请人 发明人
分类号 C07D223/12 主分类号 C07D223/12
代理机构 代理人
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