发明名称 METHOD OF PRODUCING SOLUBLE HEXAGONAL BORON NITRIDE
摘要 FIELD: chemistry.SUBSTANCE: invention relates to colloidal solutions of different nano-forms of hexagonal boron nitride (h-BN) in liquid media, and specifically to obtaining hexagonal boron nitride (h-BN) which is soluble in water and polar solvents. The method of obtaining soluble hexagonal boron nitride involves mixing hexagonal boron nitride with a functionalising agent. The reaction mixture is then heated and the obtained product is dissolved in a solvent with ultrasonic action and the solution of the end product is separated. The functionalising agent used is hydrazine or a mixture of nitric acid and sulphuric acid or oleum. The reaction mixture is dispersed by ultrasound with subsequent heating and periodic ultrasonic dispersion during heating. The process is carried out in a closed volume. The obtained product is dispersed by ultrasound in water or a polar organic solvent.EFFECT: method enables to simplify and increase efficiency of producing soluble functionalised h-BN by increasing output of soluble h-BN and using cheaper technologically acceptable functionalising agents.4 cl, 1 dwg, 3 ex
申请公布号 RU2478077(C2) 申请公布日期 2013.03.27
申请号 RU20110117429 申请日期 2011.04.29
申请人 FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE UCHREZHDENIE NAUKI INSTITUT NEORGANICHESKOJ KHIMII IM. A.V.NIKOLAEVA SIBIRSKOGO OTDELENIJA ROSSIJSKOJ AKADEMII NAUK (INKH SO RAN) 发明人 NAZAROV AL'BERT SEMENOVICH;DEMIN VIKTOR NIKOLAEVICH;FEDOROV VLADIMIR EFIMOVICH
分类号 B82B3/00;C01B21/064;C01B35/14 主分类号 B82B3/00
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