发明名称 |
Process for the production of ultra-fine zeolite crystals and their aggregates |
摘要 |
A process for producing ultra-fine zeolite nanocrystals and their aggregates having an intracrystalline void within 1~10 nanometers in size that comprises at least as follows: preparing a transparent silicate-containing aqueous solution, with optional elements as Aluminum, Titanium and organic template molecules, known to produce zeolite; heating the solution under a temperature of 25°~100° C. for a certain period of time while keeping the solution still in a transparent state without forming colloidal zeolite; adding an anionic surfactant to precipitate the inorganic components; forming the dried inorganic-organic hybrid precipitate into a desired shape and then heating the shaped body with steam under a temperature of 100°~200° C. and a relative humidity of 30~85% for 1~3 days to produce ultra-fine zeolite crystals having a size below 30 nanometers, and aggregates of ultra-fine zeolite crystals with a large number of intracrystalline voids whose size is within 1~10 nanometers.
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申请公布号 |
US6746660(B1) |
申请公布日期 |
2004.06.08 |
申请号 |
US20020316060 |
申请日期 |
2002.12.11 |
申请人 |
NATIONAL CENTRAL UNIVERSITY |
发明人 |
CHIANG ANTHONY;CHEN CHING CHUAN;NAIK SAJO P. |
分类号 |
C01B37/02;C01B39/02;C04B35/18;(IPC1-7):C01B39/02 |
主分类号 |
C01B37/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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