发明名称 SUBSTANTIALLY ANHYDROUS FOAMING AGENT AND PROCESS FOR PRODUCING THE SAME
摘要 1. A substantially anhydrous blowing agent obtained by treating a blowing agent with a surface-treating agent capable of removing water from the blowing agent in which a blowing agent is crystalline azodicarbonamide. 2. The substantially anhydrous blowing agent according to claim 1, wherein the surface-treating agent is at least one selected from the group consisting of a coupling agent, an organic acid anhydride, an anhydrous inorganic compound, and a desiccant. 3. The substantially anhydrous blowing agent according to claim 2, wherein the surface-treating agent is at least one selected from the group consisting of a silane coupling agent, an aluminum coupling agent, and a titanate coupling agent. 4. The substantially anhydrous blowing agent according to claim 3, wherein the surface-treating agent is an aluminum coupling agent, and the surface of the blowing agent is coated with aluminum hydroxide. 5. A process for producing a substantially anhydrous blowing agent, which comprises treating a blowing agent with a surface-treating agent capable of removing water from the blowing agent under conditions substantially free of a solvent, wherein the blowing agent is crystalline azodicarbonamide. 6. The process according to claim 5, wherein heating treatment is carried out during or after the treatment with the surface-treating agent. 7. The process according to claim 6, wherein the heating treatment is carried out at a temperature of 30 degree C to the decomposition temperature of the blowing agent. 8. The process according to claim 7, wherein the heating is carried out at a temperature of 55 to 100 degree C. 9. The process according to any one of claims 6 to 8, wherein the surface-treating agent is subjected to preheating treatment. 10. The process according to any one of claims 6 to 9, wherein the treatment of the blowing agent with the surface-treating agent is carried out by spraying the surface-treating agent to the blowing agent, and mixing them under mixing conditions where pulverization of a blowing agent is inhibited. 11. The process according to claim 10, wherein a ribbon blender or a screw mixer is used as a mixer under the mixing conditions where pulverization of a blowing agent is inhibited. 12. The process according to any one of claims 5 to 11, wherein the surface-treating agent is at least one selected from the group consisting of a coupling agent, an organic acid anhydride, an anhydrous inorganic compound, and a desiccant. 13. The process according to claim 12, wherein the surface-treating agent is at least one selected from the group consisting of a silane coupling agent, an aluminum coupling agent, and a titanate coupling agent. 14. The process according to claim 13, wherein the surface-treating agent is selected from the group consisting of aluminum isopropylate, aluminum ethylate, aluminum tris(ethylacetoacetate), and ethylacetoacetatoaluminum diisopropylate.
申请公布号 EA002426(B1) 申请公布日期 2002.04.25
申请号 EA20000000345 申请日期 1998.07.10
申请人 OTSUKA CHEMICAL CO., LTD 发明人 MAEKAWA, TSUKASA;SHONO, SADAFUMI;SUMITOMO, SHIGERU;UEDA, NOBUYKI;TACHI, YOSHIFUMI
分类号 C08J9/00;C08J9/10 主分类号 C08J9/00
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