发明名称 |
Process for the preparation of thioglycolic acid |
摘要 |
Preparation of thioglycolic acid (I) comprises reaction of monochloroacetic acid with hydrogen sulphide under pressure in the presence of tert. amines in solution. The novelty is that: (a) the H2S partial pressure above the reaction medium is maintained at at least 2 bars till the end of the reaction; and (b) the thioglycolic acid which is formed as its ammonium salt, is released by treatment with an acid. |
申请公布号 |
EP0780368(A1) |
申请公布日期 |
1997.06.25 |
申请号 |
EP19960119601 |
申请日期 |
1996.12.06 |
申请人 |
AKZO NOBEL N.V. |
发明人 |
BERGFELD, MANFRED JOSEF, DR.;BLAUFELDER, CHRISTIAN, DR. |
分类号 |
C07C319/02;C07C323/52 |
主分类号 |
C07C319/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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