发明名称 |
Process for the preparation of ultrapure heavy metal fluorides |
摘要 |
This invention provides a method for the preparation of ultrapure active metal fluorides of increased purity from their metal oxides by reacting an active metal with a predetermined amount of HF(aq) to form a solid reaction product which is dried under controlled heating to form a hydrated fluoride. This hydrated active metal fluoride is then subjected to reactive atmosphere processing comprising hydrofluoric acid vapor in a CO2 reactive carrier gas and a selected halide compound in the gas phase for a predetermined period of time to further increase anion purity.
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申请公布号 |
US4857293(A) |
申请公布日期 |
1989.08.15 |
申请号 |
US19870109360 |
申请日期 |
1987.10.15 |
申请人 |
HUGHES AIRCRAFT COMPANY |
发明人 |
PASTOR, RICARDO C.;GORRE, LUISA E. |
分类号 |
C01B9/08;C01G5/02;C01G13/04;C01G15/00;C01G21/16 |
主分类号 |
C01B9/08 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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