摘要 |
A process for the continuous preparation of a ditertiary butylcresol wherein m- or p-cresol is reacted with isobutene at elevated temperature using H2SO4 as catalyst wherein the process is carried out stepwise by introducing stepwise into a reaction mixture comprising substantially all of the cresol to be reacted with isobutene. The total amount of isobutene introduced is introduced such that less isobutene is charged in a last stage of the process than in the first stage thereof. Thereafter the catalyst is deactivated. |