发明名称 PURIFICATION METHOD FOR OPTICALLY ACTIVE ALPHA-TRIFLUOROMETHYL LACTATE
摘要 PROBLEM TO BE SOLVED: To provide a simple purification method for optically activeα-trifluoromethyl lactate that is useful as an effective intermediate for optically active medicine or optically active agrochemical. SOLUTION: The optically activeα-trifluoromethyl lactate that is represented by formula (I) (wherein * indicates an asymmetric carbon) is recrystallized by using one kind of solvent or a mixed solvent including plural kinds of solvents selected from the group consisting of aromatic hydrocarbon solvent, aliphatic hydrocarbon solvent, ether solvent, ester solvent, ketone solvent, acetonitrile, and N,N-dimethylformamide, then the optical purity-improved portion is collected, namely the precipitated crystal or the mother liquor residue. COPYRIGHT: (C)2007,JPO&INPIT
申请公布号 JP2007217440(A) 申请公布日期 2007.08.30
申请号 JP20070150595 申请日期 2007.06.06
申请人 MITSUBISHI RAYON CO LTD 发明人 SATO EIJI;ENOMOTO KANEHIKO;URAGAKI TOSHITAKA
分类号 C07C51/43;C07B57/00;C07C59/115 主分类号 C07C51/43
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