Process for the production of sintered aluminium nitrides.

摘要

A process for producing sintered aluminium nitride bodies comprises sintering a relatively impure aluminium nitride powder comprising at least 95% by weight aluminium nitride and having not more than 3% bound oxygen content, not more than 0.6% metal or metal compound impurities, and not more than 0.5% silicon or carbon impurities, the sintering being carried out by heating the aluminium nitride body from room temperature to the sintering temperature at a rate of not more than 250 DEG C per hour; introducing an inert gas containing from 1 to 4% by volume hydrogen until the temperature reaches 1200 DEG C; continuing to introduce solely an inert gas as the temperature is further increased to the sintering temperature; sintering the body at a sintering temperature of from 1600 DEG to 1900 DEG C; and cooling the sintered body at a rate of not more than 300 DEG C per hour.