| 摘要 |
<p>Cellulose ethers are prepared by reacting in a heterogenous reaction mixture an alkaline solution and an etherifying agent with a fibrous cellulose. The total of the required stoichiometric amount of the alkaline solution and at least a portion of the etherifying agent required in producing the cellulose ether are admixed at sufficiently low temperature to suppress reaction between the alkaline solution and the etherifying agent. The admixture is then contacted with the cellulose fibers, preferably by spraying the admixture thereupon. Additional etherifying agent is then added, if required, to the reaction mixture, and the heterogenous reaction mixture is agitated and reacted at an initial temperature below 40 DEG C, sufficient to produce alkalization of the cellulose. Thereafter the temperature is increased above 40 DEG C to produce etherification of the cellulose and form the cellulose ether.</p> |
