发明名称 PREPARATION METHOD OF NANO-SIZED HOLLOW PARTICLE BY DISPERSING STRUCTURE IN SALT SOLUTION, SPRAYING AEROSOL OBTAINED FROM THE PRODUCT, REMOVING SOLVENT AND PRECIPITATING SALT, HEATING THE PRODUCT AT SUITABLE TEMPERATURE, AND REMOVING SALT
摘要 PURPOSE: A method for preparing a nano-sized hollow particle is provided, to reduce a multi-step from the removal of structure to the post-heat treatment to a single step, to minimize the amount of waste water and to allow a hollow particle to be produced massively. CONSTITUTION: The method comprises the steps of dispersing a structure coated with an outer film in a salt solution uniformly; making aerosol from the obtained product and dispersing the aerosol in air; removing the solvent constituting the aerosol to evaporation and precipitating salts into crystal; maintaining the obtained product at a temperature where the structure can be removed and the outer film can be crystallized, to prepare a hollow particle; and removing salt from the obtained one to prepare a nano-sized hollow particle. Preferably the outer film comprises a metal oxide or a metal material; and structure comprises at least one material selected from polystyrene and PMMA; and the salt is at least one selected from the group consisting of NaCl, AlF3, BaCl2, BaF2, BeSO4, CaSO4, MgSO4, MgF2, NiF2, ScF3 and SrF2.
申请公布号 KR20050012555(A) 申请公布日期 2005.02.02
申请号 KR20030051548 申请日期 2003.07.25
申请人 KOREA ADVANCED INSTITUTE OF SCIENCE AND TECHNOLOGY 发明人 CHUNG, YUN SUP;LIM, JUNG SUN;PARK, SEUNG BIN
分类号 C08J3/12;B01J2/10;B01J13/04;B01J21/06;(IPC1-7):C08J3/12 主分类号 C08J3/12
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