摘要 |
<p>By supplying gaseous nitrogen throughout a discrete aliquot of a preferably pelletized mixture of aluminum oxide, carbon and, optionally, calcium oxide during the carbothermal reduction thereof to aluminum nitride and continuously removing gaseous reaction products therefrom, a high quality aluminum nitride is produced. One means of supplying gaseous nitrogen to the mixture of solid reactants is a perforated tray (70) having a hollowed-out bottom. Gaseous nitrogen supplied to the hollowed-out portion flows through the perforations (75) and throughout solid reactants contained in the tray. The carbon may be alternatively supplied, in whole or in part, as a gaseous reactant. <IMAGE></p> |