发明名称 Verfahren zur Reinigung von sterisch gehinderten 4-Aminopiperidinen
摘要 A process for purifying raw piperidines of formula (I), where R<1> to R<4> are C1 to C6 alkyl, R<1> and R<2> and/or R<3> and R<4> together are a CH2 chain with 2 to 5 C atoms. Said process is characterized in that in an initial step high-boiling-point substances and possible water are eliminated by distillation from the raw piperidines, in a second step 0.01 to 5 wt %, in relation to the product of the first step, of a reducing agent are added and in a third step the piperidines are isolated by distillation.
申请公布号 DE19622269(A1) 申请公布日期 1997.12.04
申请号 DE19961022269 申请日期 1996.06.03
申请人 BASF AG, 67063 LUDWIGSHAFEN, DE 发明人 JULIUS, MANFRED, DR., 67117 LIMBURGERHOF, DE;RUST, HARALD, 67435 NEUSTADT, DE;KRAUSE, ALFRED, DR., 67346 SPEYER, DE;SIEGEL, HARDO, DR., 67346 SPEYER, DE;SIEGEL, WOLFGANG, DR., 67117 LIMBURGERHOF, DE;WITZEL, TOM, DR., 67069 LUDWIGSHAFEN, DE
分类号 C07D211/58;C07D211/56;(IPC1-7):C07D213/73 主分类号 C07D211/58
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