发明名称
摘要 A method for producing high-temperature superconducting ceramic material through mechanical orientation including mixing starting materials in powdered form in proportions effective to produce a high-temperature superconducting oxide ceramic having anisotropic crystal grains and shaping the mixture. Next, the shaped mixture is calcined at a temperature ranging from 600 DEG to 900 DEG C. and fired at a temperature higher than 1,000 DEG C. in an oxygen atmosphere for a time effective to produce a superconducting oxide ceramic having crystal grains. According to the invention, the superconductive oxide ceramic is then pulverized into particles having either a plate-like form or a needle-like form based on the anisotropic form of the crystal grains. Particles of a selected size are placed into a vessel and vibrated with an acoustic vibrator means under conditions effective to cause the pulverized particles to turn toward a common preferred orientation to provide oriented particles. Then, the oriented particles are shaped by applying pressure to the vessel in a direction perpendicular to the common preferred orientation and fired at a temperature ranging from 900 DEG to 1,000 DEG C. for a time effective to produce the high-temperature superconducting oxide ceramic material with anisotropic crystal structure.
申请公布号 JPH0665623(B2) 申请公布日期 1994.08.24
申请号 JP19890062297 申请日期 1989.03.16
申请人 发明人
分类号 C04B35/00;C01B13/14;C01G1/00;C01G3/00;C04B35/45;H01B12/00;H01L39/24 主分类号 C04B35/00
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