Method of preparation of 4-aminodiphenylamine

摘要

A method of preparing 4-aminodiphylamine through an intermediate preparation of 4-nitrodiphenylamine and/or 4-nitrosodiphenylamine and/or their salts by reaction of aniline with nitobenzene in a liquid medium at a temperature of 50 to 130° C., under normal or reduced pressure, in an inert atmosphere or in the presence of air oxygen, with subsequent hydrogenation of an intermediate of 4-nitrodiphenlyamine and/or nitrosodiphenylamine and side products, and by isolation of 4-aminodiphenylamine and the side products of unconverted raw materials