发明名称 Process for preparing purified 2,6-naphthalenedicarboxylic acid
摘要 A process for preparing purified 2,6-naphthalenedicarboxylic acid which comprises hydrolyzing a dialkyl-2,6-naphthalenedicarboxylate with water at a reaction temperature of at least about 450 DEG F. under liquid phase condition, the amount of water present being sufficient to solubilize, at the reaction temperature, at least about 10 percent of the 2,6-naphthalenedicarboxylic acid formed; and a process for purifying 2,6-naphthalenedicarboxylic acid comprising combining impure 2,6-naphthalenedicarboxylic acid with a purification solvent, heating the resulting mixture under liquid phase conditions at a temperature of at least about 500 DEG F. to form a product mixture and thereafter recovering from the product mixture purified 2,6-naphthalenedicarboxylic acid.
申请公布号 US5563294(A) 申请公布日期 1996.10.08
申请号 US19940206517 申请日期 1994.03.04
申请人 AMOCO CORPORATION 发明人 HOLZHAUER, JUERGEN K.;ALBERTINS, RUSINS;HOOVER, STEPHEN V.;SIKKENGA, DAVID L.
分类号 C07C51/09;C07C51/255;C07C51/265;C07C51/42;C07C51/43;C07C51/487;C07C51/493;(IPC1-7):C07C51/09 主分类号 C07C51/09
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