发明名称 PENAM CRYSTAL AND PROCESS FOR PRODUCING THE SAME
摘要 Novel 2alpha-methyl-2beta-[(1,2,3-triazol-1-yl)methyl]penam--3alpha-carboxylic acid benzhydryl ester (TMPB)-acetone crystals for use in producing 2alpha-methyl-2beta-[(1,2,3-triazol-1-yl)-methyl]penam- 3alpha-carboxylic acid 1,1-dioxide benzhydryl ester (TAZB); a process for producing TMPB-acetone crystals which comprises (A) the step of concentrating an organic solvent solution containing TMPB, (B) the step of dissolving the resultant concentrate in acetone, and (C) the step of crystallizing TMPB-acetone crystals from the acetone solution obtained; and a process for producing TAZB which comprises the step of reacting TMPB-acetone crystals with an oxidizing agent.
申请公布号 KR20060120036(A) 申请公布日期 2006.11.24
申请号 KR20067006948 申请日期 2004.10.08
申请人 OTSUKA CHEMICAL CO., LTD.;TAIHO PHARMACEUTICAL CO., LTD. 发明人 TOKUMARU YOSHIHISA;SHIMABAYASHI AKIHIRO
分类号 C07D499/04;C07D499/87;C07D499/00;C07D499/86;C07D499/897 主分类号 C07D499/04
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