发明名称 |
MANUFACTURE OF HALOALKYL LACTAMS |
摘要 |
FDN-1532 MANUFACTURE OF HALOALKYL LACTAMS A process for the manufacture of haloalkyl lactams having the formula wherein n is an integer having a value of from 1 to 3; m is an integer having a value of 1 or 2 and X is chlorine or bromine in the absence of an inert solvent by reacting a hydroxyalkyl lactam of the formula with a thionyl chloride or bromide in the liquid phase under anhydrous conditions, vaporizing and removing any excess thionyl halide along with SO2 by-product from the liquid reaction mixture under vacuum followed by vacuum distillation of the remaining liquid product mixture at a temperature below its decomposition and recovering said product. The product of this process can be obtained in greater than 90% yield and 99% purity. 0432P |
申请公布号 |
CA1315794(C) |
申请公布日期 |
1993.04.06 |
申请号 |
CA19880559448 |
申请日期 |
1988.02.22 |
申请人 |
GAF CORPORATION |
发明人 |
TRACY, DAVID J.;RIZZO, THOMAS |
分类号 |
C07D;C07D207/26;C07D207/27;C07D211/00;C07D211/76;C07D223/10 |
主分类号 |
C07D |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|