发明名称 |
DOUBLE WALL CARBON NANOTUE AND METHOD FOR PREPARING SAME |
摘要 |
<p>PURPOSE: A double-walled carbon nanotube using a supported catalyst and a manufacturing method thereof are provided to have high purity and high selectivity of double-walled carbon nanotubes among synthesized carbon nanotubes and to reduce deformity and increase crystallinity. CONSTITUTION: A manufacturing method of double-walled carbon nanotubes comprises the following steps: preparing a supported catalyst; synthesizing carbon nanotubes by concurrently injecting hydrocarbon gas and hydrogen gas while increasing the temperature of a reactor up to 900-1000 deg. Celsius after charging the supported catalyst; and synthesizing carbon nanotubes by injecting hydrogen gas after decreasing reactor temperature to 200 deg. Celsius. The supported catalyst is manufactured by plasticizing a catalyst solution in which metallic catalysts and support elements are mixed in the reactor at 500-800 deg. Celsius. The ratio of support element (Mg): metallic catalyst (Co): molybdenum system activator (Mo) is 0 99: x: 0.025. Here, 0.05<=x<=0.075.</p> |
申请公布号 |
KR20130049737(A) |
申请公布日期 |
2013.05.14 |
申请号 |
KR20120123322 |
申请日期 |
2012.11.02 |
申请人 |
CHEIL INDUSTRIES INC. |
发明人 |
YOUM, KYOUNG TAE;KIM, BYEONG YEOL;LEE, YOUNG SIL;LIM, BO KYUNG |
分类号 |
C01B31/02;B01J6/00;B01J23/882 |
主分类号 |
C01B31/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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