发明名称 METHOD FOR PREPARING PHENYL BIS (2,4,6-TRIMETHYL BENZOYL) PHOSPHINE OXIDE
摘要 Disclosed is a method for preparing phenyl bis(2,4,6-trimethyl benzoyl) phosphine oxide as a free radical photoinitiator with high efficiency. The method specifically involves reacting phenyl phosphine as a starting material with 2,4,6-trimethyl benzoyl chloride under alkaline compounds to obtain an intermediate, and obtaining the phenyl bis(2,4,6-trimethyl benzoyl) phosphine oxide through an oxidation of the obtained intermediate. The method provided by the present invention is low-cost, easy to operate, high in yield, environmentally-friendly and adaptable to industrialization.
申请公布号 WO2016090710(A1) 申请公布日期 2016.06.16
申请号 WO2015CN00872 申请日期 2015.12.07
申请人 TIANJIN JIULIAN TECHNOLOGY CO., LTD 发明人 LIAO, WENJUN;ZHANG, LEI
分类号 C07F9/53 主分类号 C07F9/53
代理机构 代理人
主权项
地址