发明名称 PREPARATION OF AZO PIGMENTS WITH LOW PCB CONTENT BY COUPLING IN THE PRESENCE OF OLEFINS
摘要 PCT No. PCT/EP90/00955 Sec. 371 Date Feb. 21, 1992 Sec. 102(e) Date Feb. 21, 1992 PCT Filed Jun. 16, 1990 PCT Pub. No. WO90/15844 PCT Pub. Date Dec. 27, 1990.The production which is customary in practice of monoazo compounds based on dichloro- and trichloroanilines or disazo compounds of the chlorinated biphenyl series by conventional coupling methods meets with difficulties in that the resulting pigments are contaminated by traces of polychlorinated biphenyls. According to the invention, it has now been found that by addition of water-soluble olefins of the type <IMAGE> (R =H, alk or Oalk; X =-COOR1, -CONHR2 or -NR3COR4) in the azo coupling, the side reactions which form PCBs can be decidedly suppressed during synthesis of the pigments.
申请公布号 US5243032(A) 申请公布日期 1993.09.07
申请号 US19920781257 申请日期 1992.02.21
申请人 HOECHST AKTIENGESELLSCHAFT 发明人 RIEPER, WOLFGANG
分类号 C09B41/00;C09D7/12;C09D11/00;C09D11/02 主分类号 C09B41/00
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