METHOD OF SYNTHESIS OF 2,2-DI-(TERTIARY-BUTYLPEROXY)-BUTANE

摘要

organic chemistry, chemical technology. SUBSTANCE: invention relates to method of synthesis of 2,2-di-(tert.-butylperoxy)-butane that is used as an initiating agent of polymerization process in synthesis of polymers, addition agent to diesel fuel and improving its spontaneous combustibility. Process is carried out in the presence of magnesium sulfate dihydrate in the following ratio of the parent components: tert.-butyl hydroperoxide : methylethyl ketone : : hydrochloric acid : magnesium sulfate dihydrate = 1:(0.5- 0.7):(0.07-0.21):(0.20-26), respectively. EFFECT: increased conversion of parent raw, improved quality of product. 1 tbl, 7 ex