VERFAHREN ZUM HERSTELLEN EINER VERSTÄRKENDEN SIC-FASER FÜR SIC-VERBUNDWERKSTOF FMATERIAL
摘要
A mixed polymer liquid is prepared by mixing a polycarbosilane-dissolved organic solvent with poly(methylsilane) and moderated to viscosity of 5-20 Pa.s by heat-treatment to promote partial cross-linking reaction. The mixed-polymer is then melt-spun to fiber at 250-350 DEG C. The fiber is cured by treatment at 100-200 DEG C in an oxidizing atmosphere, and baked at 1000 DEG C or higher. Due to thermosetting action of poly(methylsilane), the mixed polymer liquid is continuously melt-spun without breakage, and SiC fiber produced in this way is useful for reinforcement of SiC composite excellent in toughness, strength and heat-resistance.